糖的洗脱体积

2023-07-12 7

色谱柱DC-613 (RSpak);GS-220 HQ (Asahipak);KS-801 (SUGAR);NH2P-50 4E (Asahipak);SC1011 (SUGAR);SC1211 (SUGAR);SP0810 (SUGAR);SZ5532 (SUGAR); 1-Fructofuranosyl-D-nystose 1-呋喃果糖基-D-蔗果四糖;1-Kestose 1-酮糖;2-Deoxy-D-glucose 2-脱氧-D-葡萄糖;4'-Galactosyllactose 4'-半乳糖;meso-Erythrito l赤藓糖醇;myo-Inositol肌苷醇;Arabinose树胶醛糖;Arabitol 阿拉伯糖醇;Aspartame 阿斯巴甜;Difructoseanhydride III 二果糖酸酐III;Ethanol, Ethyl alcohol乙醇;Fructose果糖;

七种不同色谱柱SUGAR SP0810, SC1011, KS-801, SZ5532, SC1211, RSpak DC-613, Asahipak NH2P-50 4E和GS-220 HQ 对糖的洗脱体积见下表。表中只提供了出峰的位置,如果希望看到实际的色谱峰宽,请和我们联系。  
(-) -> 未检出 (*) -> 与溶剂峰重叠
Columns:Shodex SUGAR SP0810, SC1011, KS-801 (8.0 mm I.D. x 300 mm each)
Eluent:H2O
Flow rate:1.0 mL/min
Detector:RI
Column temp.:80 ℃
Column:Shodex SUGAR SZ5532 (6.0 mm I.D. x 150 mm)
Eluent:H2O/CH3CN=25/75
Flow rate:1.0 mL/min
Detector:RI
Column temp.:60 ℃
Column:Shodex SUGAR SC1211 (6.0 mm I.D. x 250 mm)
Eluent:H2O/CH3CN=65/35
Flow rate:1.0 mL/minv
Detector:RI
Column temp:70 ℃
Column:Shodex RSpak DC-613 (6.0 mm I.D. x 150 mm)
Eluent:H2O/CH3CN=25/75
Flow rate:1.0 mL/min
Detector:RI
Column temp.:70 ℃
Column:Shodex Asahipak NH2P-50 4E (4.6 mm I.D. x 250 mm)
Eluent:H2O/CH3CN=25/75
Flow rate:1.0 mL/min
Detector:RI
Column temp:30 ℃
Columns:Shodex Asahipak GS-220 HQ (7.5 mm I.D. x 300 mm) x 2
Eluent:H2O
Flow rate:0.5 mL/min
Detector:RI
Column temp:60 ℃
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